产品介绍：
产品说明
应用
Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets
Each kit contains 2 customizable screening sets that include the following components:
- 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
- 4 x 4 mL reaction vials with pre-weighed KOAc
- Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
- 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
- 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
- 4 stir bars for substrate stock solution vials.
- 1 internal standard.
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
特点和优势
- Designed and tested by synthetic chemists.
- Easily run 24-microscale reactions in parallel.
- 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.
法律信息
KitAlysis is a trademark of sigma-aldrich Co. LLC
产品性质
| reaction suitability | reaction type: Buchwald-Hartwig Cross Coupling Reaction reaction type: Cross Couplings reaction type: Heck Reaction reaction type: Hiyama Coupling reaction type: Negishi Coupling reaction type: Sonogashira Coupling reaction type: Stille Coupling reaction type: Suzuki-Miyaura Coupling reagent type: catalyst core: palladium |
| 官能团 | phosphine |
组份列表
组份可单独销售
| 货号 | 组份 |
| 764175 | P(Cy3) Pd G3, 97% |
| 791733 | Potassium acetate, anhydrous, free-flowing, Redi-Dri™, ACS reagent, ≥99.0% |
| 804274 | XPhos Pd G4, 95% |
| 804282 | SPhos Pd G4 |
| 804290 | RuPhos Pd G4 |
| 804975 | DTBPF-Pd-G3 |
| 900349 | cataCXium Pd G4 |
| 900522 | Toluene, anhydrous, ZerO2®, 99.8% |
| 900631 | Ethylene glycol, anhydrous, ZerO2®, 99.8% |
| 900634 | N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% |
| 900636 | Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% |
| 900639 | 1-Butanol, anhydrous, ZerO2®, 99.8% |
| 900641 | Methanol, anhydrous, ZerO2®, 99.8% |
| 900644 | Acetonitrile, anhydrous, ZerO2®, 99.8% |
| 900690 | N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5% |
| 221171 | Pinacol, 98% |
| 473294 | Bis(pinacolato)diboron, 99% |
| 754242 | Tetrahydroxydiboron, 95% |
| B34656 | Biphenyl, ReagentPlus®, 99.5% |
| Z118850 | Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm |
| Z742110 | KitAlysis™ 24-well reaction block replacement film |
安全信息
| 象形图 |      |
| 警示用语： | Danger |
| 危险声明 | H225 - H301 + H311 + H331 - H315 - H318 - H335 - H336 - H351 - H360D - H370 - H373 - H410 |
| 预防措施声明 | P210 - P273 - P280 - P301 + P310 - P303 + P361 + P353 - P305 + P351 + P338 |
| 危险分类 | Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1 |
| 靶器官 | Kidney |
| 补充剂危害 | EUH019 |
| 储存分类代码 | 3 - Flammable liquids |
| WGK | WGK 3 |
| 闪点(F) | 1.4 °F |
| 闪点(C) | -17 ℃ |
